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100L Simple Distillation Short Path Distillation Apparatus

100L Simple Distillation Short Path Distillation Apparatus

1. Vacuum Low-Temperature Purification for Heat-Sensitive High-Boiling Materials
2. GG17 Glass + Full PTFE Wetted Parts, Clean and Corrosion-Resistant
3. 50–450 rpm Magnetic Stirring, 400W Geared Motor, Steady-State Long-Term Operation
4. 15 kW Jacket Heating, RT–180℃ Constant Temperature Control, Frame 304 Stainless Steel.

Product Introduction

 

Products Description

simple distillation, Short Path Distillation

Short path (simple) distillation is a novel separation technology capable of addressing challenges beyond the scope of conventional distillation methods. It enables "liquid-liquid" separation under vacuum conditions at temperatures significantly below the boiling point of liquids. This technique is particularly well-suited for the separation and purification of high-boiling-point, heat-sensitive, and oxidation-prone materials.

The 100 L TDS-100L is perfect for scale-up when the available space and budget are limited.

 

 

Key Advantages

 

■Variable-frequency speed control, high-power magnetic stirring device with constant rotation speed. Brushless, spark-free, safe and stable, capable of sustained long-term operation.


■Complete glassware set manufactured from GG17 or G3.3 high borosilicate glass, offering excellent chemical and physical properties.


■PTFE and rubber composite seals maintain high vacuum levels, ensuring a vacuum up to 0.095 MPa.


■Integrated design for reaction, heating, stirring, reflux, and distillation. Compared to similar equipment, it occupies a smaller footprint and offers high cost-effectiveness.


■Intelligent electric heating with constant temperature control delivers excellent insulation. The temperature range spans from room temperature to 180°C.


■Heating system controlled by solid-state relay assemblies ensures spark-free operation, minimal interference, and extended service life.


■Reaction materials come into contact only with GG17 glass and fully PTFE components, guaranteeing contamination-free processing.

 

Specifications

 

Product Model

TDS-100L

Material Capacity

100L

Glass Material

High borosilicate GG17

Distillation kettle

Number of openings

Distillation port

   

Feed inlet

   

Temperature measurement port

   

Spare port

 

Mixing Method

Magnetic stirrer

 

Mixing Power

400W geared motor

 

Mixing Control

Digital display control

 

Mixing Speed

Electric stirring 50-450rpm

 

Heating Method

Heating jacket bath pot heating

 

Heating Power

15KW

 

Operating Temperature

RT-180℃

 

Temperature Sensor

PT100

Collection vessel

Number of openings

Feed inlet

   

Standby inlet

   

Bottom discharge outlet

Instrument Fixture

1 set

Mobile Casters

With brakes

Complete Unit Frame

Stainless steel 304 lattice frame

Complete Unit Power Supply

380V

 

Shipment Images

 

simple distillation, Short Path Distillation

100Lsimple distillation, Short Path Distillation

100L simple distillation, Short Path Distillation

100Lsimple distillation, Short Path Distillation

100L simple distillation, Short Path Distillation

100L simple distillation, Short Path Distillation

100L Heatingand coinng crulators

100L Heatingand coinng crulators

Applications

 

★ Thermal separation of heat-sensitive compounds
★ Purification of organic synthetic substances
★ Isolation of active components from biological extracts
★ Recycling of industrial waste materials
★ Removal of toxic contaminants in the food industry
★ Decolorization and deodorization of organic compounds
★ High-precision removal of residual solvents from compounds

 

Customization 

The customization scope for short-path molecular distillation equipment is extensive, covering multiple aspects including materials, specifications, feed/discharge methods, film-forming technology, temperature control systems, and automation levels. Users can select appropriate configurations based on specific applications (e.g., pharmaceuticals, chemicals, food) and material characteristics (e.g., heat sensitivity, high viscosity).
For more detailed technical solutions, we recommend contacting TOPTION directly for tailored designs.

simple distillation, Short Path Distillation

 

Certificate

 

Short-path distillation equipment certificate

 

About Us

 

product-750-623

product-750-732

product-750-747

 

FAQ

 

Q1: Can molecular distillation separate two compounds with very close boiling points?
A1: It is challenging, but possible. For example, to raise the ethyl palmitate: palmitic acid ratio from 9:1 to 96% purity, about 10–20% of the material must be distilled out. Customers are encouraged to send samples for feasibility testing.

 

Q2: What is the molecular distillation process for biodiesel?
A2:

Using two-stage molecular distillation, yields range between 85%–90%.

With four stages, yields improve to 90%–95%.

With six stages, yields can reach 93%–96%.

 

Q3: What is the difference between simple distillation and short-path distillation?
A3:

For separating conventional, stable liquids with large differences in boiling points, simple distillation is the preferred choice due to its simplicity and low cost.

When handling high-boiling-point, heat-sensitive, oxygen-sensitive precious substances that decompose easily upon heating, short-path distillation becomes an indispensable, powerful tool-despite its higher equipment and operational costs.
 

 

Q4: Is the 100L glass simple short-path system compatible with vacuum pumps and refrigeration units?
A4: Yes, we have compatible heating and cooling circulation pumps and refrigeration units.

 

Q5: How is MCT oil extracted from coconut oil?
A5: The common industrial method includes hydrolysis, rectification, and esterification. The esterified MCT oil is then purified through molecular distillation for high-quality results.

 

Help FAQ

 

 

Testing the stirring performance of a 100L simple short-path distillation apparatus

 

 

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Hot Tags: simple distillation, Short Path Distillation, simple distillation apparatus,100L short path, TDS-100L, molecular distillation apparatus

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